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Broken or shattered glass found at a crime scene is an important piece of forensic evidence. The different types of glass that are often found, such as glass from a window, lamp, headlights, or bottles, each have unique properties that can be measured and compared. When glass is shattered by a forceful impact, it scatters for distances up to nine feet or so, and can easily become lodged in a suspect's shoes, clothing, or hair. If a window or glass object is broken or shattered by a projectile, such as a bullet, the breakage pattern can be analyzed to possibly determine the angle of trajectory of the projectile, shedding more light on the crime, such as where the suspect was when the gun was fired.
Before any samples are taken, the entire scene should be photographed in detail. Tape measures can be used in the photographs to show the distances that the broken glass has traveled. Searching for nearby suspects is of primary importance, as any glass fragments that are retained on their clothing, hair, shoes, or similar will be more likely to fall off as time passes and will probably be gone after about 24 hours.
Samples of glass should be collected from the representative source (i.e., the broken window) and also from fragments of glass that are lying on the ground, floor, or furniture. All samples must be labeled according to where they came from (the original window, a broken fragment on the floor, the inside of the window, the outside, etc.). All the glass fragments should be collected and labeled so that reconstructions can be made if desired. If a suspect is found, samples should be taken from their clothing or hair for comparison. These may be microscopic.
All samples should be dry when collected. If fragments are wet, they should be allowed to air dry before being packaged. For small fragments, it is important to use containers that are not too large so that the glass doesn't bounce around and break further. Samples of glass should not be put in glass vials, but cardboard boxes, paper bindles, or envelopes of some kind should be used. These are less likely to alter the sample. Any tape that is used for sample collection should be low-adhesive so it does not adhere to itself.
Refractive index (RI) is a unique property of any type of glass that can be used to compare a sample to a source, such as a broken window in someone's home. Databases of many RI values for various glasses exist in the industry. But often, glass samples found at crime scenes are very small, so it's difficult to measure this parameter directly. For this reason, techniques are used in which the sample is immersed in a liquid of known RI, and if the sample seems to disappear, then its RI matches that of the liquid. This is one way to tell whether a sample matches an original source, like a broken window.
A glass sample can be visualized under a microscope to determine its unique surface features, such as finishes, patterns, dents, grooves, or similar traits. This is a simple way of determining whether a sample matches a representative source.
Broken glass at a crime scene is a very important type of forensic evidence. Different types of glass from different sources, such as windows, bottles, or headlights, have unique chemical and physical properties that can be measured and compared.
The initial crime scene assessment is very important in determining whether relevant information will be collected or missed. Detailed photographs of the entire scene must be taken before any samples are collected, and tape measures can be used to indicate distances that shattered glass fragments have traveled. Searching for any suspects who may have glass samples on their clothing or in their hair begin immediately, as this kind of evidence is often gone after the first 24 hours.
Sampling and packaging of glass samples must be done with great care. Samples should be kept dry and be placed in containers of appropriate size and material. Representative samples of all sources of fragments should also be taken.
Forensic glass samples can be analyzed by comparing the refractive index of the sample to that of the possible source. Examination of samples under a regular microscope or a scanning electron microscope can give detailed information about the sample's physical and chemical characteristics.
In my pain, God opened my eyes to the reality that His plans reach far beyond what my fallible eyes can see. He overwhelmed my heart with love for moms and dads who, like me, face shattered dreams of their own. He infused me with hope that perhaps my pain could be the very thing that draws me into a deeper, sweeter fellowship with Him and with others facing a similar heartache.
My recent entries in this category have, for the most part, been hazardous in a direct (not to say crude, or even vulgar) manner. These are compounds that explode with bizarre violence even in laughably small amounts, leaving ruined equipment and shattered nerves in their wake. No, I will not work with such.But today's compound makes no noise and leaves no wreckage. It merely stinks. But it does so relentlessly and unbearably. It makes innocent downwind pedestrians stagger, clutch their stomachs, and flee in terror. It reeks to a degree that makes people suspect evil supernatural forces. It is thioacetone.Or something close to it, anyway. All we know for sure is that thioacetone doesn't like to exist as a free compound - it's usually tied up in a cyclic thioketal trimer, when it's around at all. Attempts to crack this to thioacetone monomer itself have been made - ah, but that's when people start diving out of windows and vomiting into wastebaskets, so the quality of the data starts to deteriorate. No one's quite sure what the actual odorant is (perhaps the gem-dimercaptan?) And no one seems to have much desire to find out, either.There are sound historical reasons for this reluctance. The canonical example (Chemische Berichte 1889, 2593) is the early work in the German city of Freiburg in 1889 (see here), which quotes the first-hand report. This reaction produced"an offensive smell which spread rapidly over a great area of the town causing fainting, vomiting and a panic evacuation.". An 1890 report from the Whitehall Soap Works in Leeds refers to the odor as "fearful", and if you could smell anything through the ambient conditions in a Leeds soap factory in 1890, it must have been.The compound shows up sporadically in the literature until the mid-1960s, when several groups looked into thioketones as sources of new polymers. The most in-depth analysis took place at the Esso Research Station in Abingdon, UK, where Victor Burnop and Kenneth Latham got to experience the Freiburg Horror for themselves:
On the ground moments before the blast it was a calm and sunny Monday morning. An air raid alert from earlier that morning had been called off after only a solitary aircraft was seen (the weather plane), and by 8:15 the city was alive with activity -- soldiers doing their morning calisthenics, commuters on foot or on bicycles, groups of women and children working outside to clear firebreaks. Those closest to the explosion died instantly, their bodies turned to black char. Nearby birds burst into flames in mid-air, and dry, combustible materials such as paper instantly ignited as far away as 6,400 feet from ground zero. The white light acted as a giant flashbulb, burning the dark patterns of clothing onto skin (right) and the shadows of bodies onto walls. Survivors outdoors close to the blast generally describe a literally blinding light combined with a sudden and overwhelming wave of heat. (The effects of radiation are usually not immediately apparent.) The blast wave followed almost instantly for those close-in, often knocking them from their feet. Those that were indoors were usually spared the flash burns, but flying glass from broken windows filled most rooms, and all but the very strongest structures collapsed. One boy was blown through the windows of his house and across the street as the house collapsed behind him. Within minutes 9 out of 10 people half a mile or less from ground zero were dead. 2ff7e9595c
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